HRID1037690

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID8900

Heptane

C7H16

反应SMILES：CC(C)(C)NS(=O)(=O)c1ccccc1-c1ccc2nc(N)nc(C(=O)N3Cc4ccccc4C3)c2c1

HCID46701754

未命名化合物

PRODUCTS

产物

反应SMILES：Nc1nc(C(=O)N2Cc3ccccc3C2)c2cc(-c3ccccc3S(N)(=O)=O)ccc2n1

HCID46701755

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID6422

未命名化合物

CONDITIONS

反应条件

温度: 22 °C

PROCEDURE

实验过程

1 g of 2-[2-amino-4-(1,3-dihydroisoindole-2-carbonyl)quinazolin-6-yl]-N-tert-butylbenzenesulfonamide is dissolved in 10 ml of trifluoroacetic acid and stirred at 22° C. for 16 h. 10 ml of n-heptane are subsequently added and evaporated to dryness in vacuo. The crude product obtained in this way is purified by column chromatography.

WORKUP

后处理

customevaporated to dryness in vacuo