HRID1038005

反应详情

EQUATION

反应方程式

HRID 1038005 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

To a suspension of compound 55 (65 mg) in 5 mL of methanol was added catalytic amount of 5% palladium on carbon. The mixture was stirred under a hydrogen atmosphere at room temperature for 4 hrs and filtered through celite. The filtrate was concentrated to afford compound 56 (59 mg).

WORKUP

后处理

  1. filtrationfiltered through celite
  2. concentrationThe filtrate was concentrated