戻る
化工社化工社 化学情報印刷レポート · 研究参考用
HRID 1038005作成日:2026年10月25日

N-methyl-5-nitro-1H-indazole-3-carboxamide → 5-Amino-N-methyl-1H-indazole-3-carboxamide

https://huagongshe.com/reaction/1038005

反応式

関与物質

役割名称HCID仕込み量
反応物N-methyl-5-nitro-1H-indazole-3-carboxamideHCID 45810073—
触媒PalladiumHCID 23938—
溶媒MethanolHCID 887—
生成物5-Amino-N-methyl-1H-indazole-3-carboxamideHCID 22567319105.1%

反応手順

To a suspension of compound 55 (65 mg) in 5 mL of methanol was added catalytic amount of 5% palladium on carbon. The mixture was stirred under a hydrogen atmosphere at room temperature for 4 hrs and filtered through celite. The filtrate was concentrated to afford compound 56 (59 mg).

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US08546404B2
出典データセットuspto-grants-2013_10
ORD IDord-7008f161220d40e19af52abfa231e6b5
出典メモuspto-grants-2013_10