HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cesium carbonate → HCID 86614439, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cesium carbonate | HCID 10796 | — |
| Reactant | HCID 58946437 | HCID 58946437 | — |
| Reactant | HCID 86614438 | HCID 86614438 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 86614439 | HCID 86614439 | — |
Reaction Steps
Added Cesium carbonate (60 mg, 0.184 mmol) to a solution of 3-(1-Hydroxy-ethyl)-pyrrolidine-3-carboxylic acid [3-(4-fluoro-phenyl)-1Trityl-indazol-5-yl]-amide (6N) (60 mg, 0.098 mmol) and 2-chloro-1-[4-(4-pyrimidin-2-yl-phenyl)-piperazin-1-yl]-ethanone (50 mg, 0.158 mmol) in DMF (2 ml) at room temperature, then stirred overnight.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08546404B2 |
| Source dataset | uspto-grants-2013_10 |
| ORD ID | ord-ec3ea0937fb244ceb47f834f19344d45 |
| Source note | uspto-grants-2013_10 |