HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl isothiocyanatoformate → Ethyl (((5-bromo-6-methylpyridin-2-yl)amino)carbonothioyl)carbamate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl isothiocyanatoformate | HCID 85320 | — |
| Reactant | 2-Pyridinamine, 5-bromo-6-methyl- | HCID 170678 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | Ethyl (((5-bromo-6-methylpyridin-2-yl)amino)carbonothioyl)carbamate | HCID 59437446 | — |
Reaction Steps
Ethoxycarbonylisothiocyanat (7.71 g) was added to a stirred solution of 5-bromo-6-methylpyridin-2-amine (10.0 g) in dioxane (90 ml). The mixture was stirred for 2 h at r.t. A white solid precipitated. Hexane (100 ml) was added and the white solid was collected by filtration.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08551980B2 |
| Source dataset | uspto-grants-2013_10 |
| ORD ID | ord-52e46e09fa4e4de386e15e52969ef379 |
| Source note | uspto-grants-2013_10 |