HuagongsheHuagongshe Chemistry Print Report · For research reference only
(4-Chlorophenyl)methanesulfonyl chloride → HCID 67023880, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (4-Chlorophenyl)methanesulfonyl chloride | HCID 227304 | — |
| Reactant | tert-Butyl 3-amino-5-(3,5-dicyano-2,6-dimethyl-1,4-dihydropyridin-4-yl)-1H-indazole-1-carboxylate | HCID 24959832 | — |
| Product | HCID 67023880 | HCID 67023880 | — |
Reaction Steps
The title compound was prepared following the procedure described for Example 6 starting from 100 mg (0.256 mmol) tert-butyl 3-amino-5-(3,5-dicyano-2,6-dimethyl-1,4-dihydropyridin-4-yl)-1H-indazole-1-carboxylate (Example 3A) and 346 mg (1.54 mmol) (4-chlorophenyl)methane-sulfonyl chloride. Yield: 4 mg (3% of th.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08551989B2 |
| Source dataset | uspto-grants-2013_10 |
| ORD ID | ord-6bd97dedbd33414e9c00dbe1aa0b34fe |
| Source note | uspto-grants-2013_10 |