HuagongsheHuagongshe Chemistry Print Report · For research reference only
N,N-Diethyl-p-phenylenediamine → HCID 57710357, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N,N-Diethyl-p-phenylenediamine | HCID 7120 | — |
| Reactant | 6-chloro-N-methylpyrimidin-4-amine | HCID 309479 | — |
| Product | HCID 57710357 | HCID 57710357 | — |
Reaction Steps
The title compound is prepared analogously as described in Example 105A from (6-chloro-pyrimidin-4-yl)-methyl-amine and 4-amino-N,N-diethylaniline. The ethyl acetate layer is dried over Na2SO4 and evaporated in vacuo. The residue is suspended in CH2Cl2, filtered off and dried to afford the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08552002B2 |
| Source dataset | uspto-grants-2013_10 |
| ORD ID | ord-3c236ae5c4004f63a5ee7b8193ec5493 |
| Source note | uspto-grants-2013_10 |