1,3-Dichloro-2-isocyanatobenzene → HCID 57710249, compound

HRID 1038695Notes

Reaction equation

HRID 1038695 reaction equation
[CH3:1][N:2]([CH3:17])[C:3]1[CH:4]=[C:5]([NH:9][C:10]2[CH:15]=[C:14]([NH2:16])[N:13]=[CH:12][N:11]=2)[CH:6]=[CH:7][CH:8]=1.[Cl:18][C:19]1[CH:24]=[CH:23][CH:22]=[C:21]([Cl:25])[C:20]=1[N:26]=[C:27]=[O:28]>C(OCC)(=O)C>[Cl:18][C:19]1[CH:24]=[CH:23][CH:22]=[C:21]([Cl:25])[C:20]=1[NH:26][C:27]([NH:16][C:14]1[CH:15]=[C:10]([NH:9][C:5]2[CH:6]=[CH:7][CH:8]=[C:3]([N:2]([CH3:17])[CH3:1])[CH:4]=2)[N:11]=[CH:12][N:13]=1)=[O:28]

Participants

4

Reactant 2

HCID 6045371,3-Dichloro-2-isocyanatobenzeneHCID 66669910HCID 66669910, compound

Product 1

HCID 57710249HCID 57710249, compound

Reagents, catalysts & solvents 1

HCID 8857Ethyl AcetateSolvent

Procedure

The title compound is prepared analogously as described in Example 105B from N-(3-dimethylamino-phenyl)-pyrimidine-4,6-diamine and 2,6-dichlorophenyl isocyanate using ethyl acetate instead of CH2Cl2 for the work-up procedure.

Sources & evidence

ORD record
ord-37e27279deab457bb78867498c01e2df
Source dataset
uspto-grants-2013_10
Patent number
US08552002B2

Reaction notes

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