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HRID1038926

反应详情

EQUATION

反应方程式

HRID 1038926 的结构方程式

REACTANTS

反应物

2
结构：O=Cc1ccccn1
HCID14273

2-Pyridinecarboxaldehyde

C6H5NO

结构：Cc1nc2ccccc2c(=O)n1-c1ccccc1
HCID63378

4(3H)-Quinazolinone, 2-methyl-3-phenyl-

C15H12N2O

PRODUCTS

生成物

1
结构：O=c1c2ccccc2nc(C=Cc2ccccn2)n1-c1ccccc1
HCID2988171

未命名化合物

收率 52%

PROCEDURE

实验过程

The title compound was synthesized according to General Procedure B using picolinaldehyde and compound 27. After cooling, the precipitate formed was filtered off, washed with water, dried and recrystallized from ethanol to yield compound 43 (0.49 g, 52%). M. Wt. 325. LCMS [M+H]+=326.

WORKUP

后处理

  1. customThe title compound was synthesized
  2. temperatureAfter cooling
  3. customthe precipitate formed
  4. filtrationwas filtered off
  5. washwashed with water
  6. customdried
  7. customrecrystallized from ethanol