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HRID1038933

反应详情

EQUATION

反应方程式

HRID 1038933 的结构方程式

REACTANTS

反应物

3
结构：COc1cccc(C=O)c1O
HCID8991

2-Hydroxy-3-methoxybenzaldehyde

C8H8O3

结构：Cc1nc2ccccc2c(=O)n1-c1ccccc1
HCID63378

4(3H)-Quinazolinone, 2-methyl-3-phenyl-

C15H12N2O

结构：CC(=O)[O-].[Na+]
HCID517045

Sodium Acetate

C2H3NaO2

PRODUCTS

生成物

1
结构：O=c1c2ccccc2nc(C=Cc2cccc(O)c2O)n1-c1ccccc1
HCID136400711

未命名化合物

收率 80.5%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CC(=O)O
溶剂HCID176

Acetic Acid

C2H4O2

PROCEDURE

实验过程

A mixture of compound 27 (0.7 g, 003 mol), 9 (0.64 g, 0.004 mol) and NaOAc (0.233 g, 0.002 mol) in AcOH was heated under reflux for 10 hours. After cooling, the precipitate formed was washed with water, dried and recrystallized from EtOH to yield 75 (0.85 g, 75%).

WORKUP

后处理

  1. temperaturewas heated
  2. temperatureunder reflux for 10 hours
  3. temperatureAfter cooling
  4. customthe precipitate formed
  5. washwas washed with water
  6. customdried
  7. customrecrystallized from EtOH