HuagongsheHuagongshe Chemistry Print Report · For research reference only
o-Vanillin → HCID 136400711, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | o-Vanillin | HCID 8991 | — |
| Reactant | 4(3H)-Quinazolinone, 2-methyl-3-phenyl- | HCID 63378 | — |
| Reactant | Sodium Acetate | HCID 517045 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 136400711 | HCID 136400711 | 80.5% |
Reaction Steps
A mixture of compound 27 (0.7 g, 003 mol), 9 (0.64 g, 0.004 mol) and NaOAc (0.233 g, 0.002 mol) in AcOH was heated under reflux for 10 hours. After cooling, the precipitate formed was washed with water, dried and recrystallized from EtOH to yield 75 (0.85 g, 75%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08552009B2 |
| Source dataset | uspto-grants-2013_10 |
| ORD ID | ord-4701a7882052427e8cbaff8f43950bf8 |
| Source note | uspto-grants-2013_10 |