Lithium hydroxide, monohydrate → HCID 57572049, compound

HRID 1039697Notes

Reaction equation

HRID 1039697 reaction equation
[CH3:1][O:2][CH:3]([CH2:8][CH3:9])[C:4]([O:6]C)=[O:5].O.[OH-].[Li+:12]>CO.O>[CH3:1][O:2][CH:3]([CH2:8][CH3:9])[C:4]([O-:6])=[O:5].[Li+:12]

Participants

5

Reactant 2

HCID 168937Lithium hydroxide, monohydrateHCID 19792887Methyl 2-methoxybutanoate

Product 1

HCID 57572049HCID 57572049, compound

Reagents, catalysts & solvents 2

HCID 887MethanolSolventHCID 962WaterSolvent

Procedure

In a 15-mL RBF was dissolved methyl 2-methoxybutanoate (0.027 g, 0.20 mmol) in methanol (0.75 mL). A solution of lithium hydroxide monohydrate (0.0086 g, 0.20 mmol) in water (0.75 mL) was added, and the mixture was stirred overnight. The mixture was concentrated to afford the title compound.

Workup

  1. concentrationThe mixture was concentrated

Sources & evidence

ORD record
ord-dbe1d2e4fede471e8bd6d9419f35581f
Source dataset
uspto-grants-2013_10
Patent number
US08552181B2

Reaction notes

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