Hydrochloric Acid → HCID 58431097, compound

Participants

Reaction Steps

To a solution of [1-(1H-Pyrrolo[2,3-b]pyridin-6-yl)-propyl]-carbamic acid tert-butyl ester (230 mg, 0.84 mmol) in dioxane (2 mL) was added 4N HCl in dioxane (500 uL, 2.00 mmol). The reaction was stirred at room temperature for 1 h. Solvents were removed and the resulting brown oil was suspended in Toluene (3 mL×2). Removal of solvents to dryness affords 197 mg of the title compound 1-(1H-Pyrrolo[2,3-b]pyridin-6-yl)-propylamine as a HCl salt, m/z 176.40 [M+1]+.

Provenance & Evidence