Sodium Carbonate → HCID 86660576, compound

Participants

Reaction Steps

The compounds are made substantially as described in Example 2A above, using appropriate substitutions of starting materials (138.6 g of 1,3-dichloro-2-propan-2-yloxydecane, 112.5 g of sodium sulfite, 39.0 g of sodium meta-bisulfite, 34.52 g of sodium carbonate, 550.43 g of water, 190° C., 20 hours). Following reaction, the reaction mixture is cooled to ambient temperature and unloaded to afford 826.5 g of light brown reaction product.

Provenance & Evidence