Sodium Carbonate → HCID 86660576, compound

HRID 1041842Notes

Reaction equation

HRID 1041842 reaction equation
Cl[CH2:2][CH:3]([O:13][CH:14]([CH3:16])[CH3:15])[CH:4](Cl)[CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH3:11].[S:17]([O-:20])([O-:19])=[O:18].[Na+:21].[Na+].[S:23](S([O-])=O)([O-:26])(=[O:25])=[O:24].[Na+].[Na+].C(=O)([O-])[O-].[Na+].[Na+]>O>[CH3:2][CH:3]([O:13][CH:14]([CH2:16][S:23]([O-:26])(=[O:25])=[O:24])[CH2:15][S:17]([O-:20])(=[O:19])=[O:18])[CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH3:11].[Na+:21].[Na+:21]

Participants

6

Reactant 4

HCID 10340Sodium CarbonateHCID 24437Sodium SulfiteHCID 656671Sodium PyrosulfiteHCID 86660578HCID 86660578, compound

Product 1

HCID 86660576HCID 86660576, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

The compounds are made substantially as described in Example 2A above, using appropriate substitutions of starting materials (138.6 g of 1,3-dichloro-2-propan-2-yloxydecane, 112.5 g of sodium sulfite, 39.0 g of sodium meta-bisulfite, 34.52 g of sodium carbonate, 550.43 g of water, 190° C., 20 hours). Following reaction, the reaction mixture is cooled to ambient temperature and unloaded to afford 826.5 g of light brown reaction product.

Workup

  1. customreaction
  2. customto afford 826.5 g of light brown reaction product

Sources & evidence

ORD record
ord-ae702121643f476db6d2507da98b666b
Source dataset
uspto-grants-2013_10
Patent number
US08557756B2

Reaction notes

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