Sodium Carbonate → HCID 86660579, compound

HRID 1041843Notes

Reaction equation

HRID 1041843 reaction equation
Cl[CH2:2][CH:3]([O:15][CH:16]([CH3:18])[CH3:17])[CH:4](Cl)[CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH3:13].[S:19]([O-:22])([O-:21])=[O:20].[Na+:23].[Na+].[S:25](S([O-])=O)([O-:28])(=[O:27])=[O:26].[Na+].[Na+].C(=O)([O-])[O-].[Na+].[Na+]>O>[CH3:2][CH:3]([O:15][CH:16]([CH2:18][S:25]([O-:28])(=[O:27])=[O:26])[CH2:17][S:19]([O-:22])(=[O:21])=[O:20])[CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH3:13].[Na+:23].[Na+:23]

Participants

6

Reactant 4

HCID 10340Sodium CarbonateHCID 24437Sodium SulfiteHCID 656671Sodium PyrosulfiteHCID 86660581HCID 86660581, compound

Product 1

HCID 86660579HCID 86660579, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

The compounds are made substantially as described in Example 2A above, using appropriate substitutions of starting materials (135.5 g of 1,3-dichloro-2-propan-2-yloxydodecane, 98.66 g of sodium sulfite, 34.18 g of sodium meta-bisulfite, 30.66 g of sodium carbonate, 590 g of water, 200° C., 20 hours). Following reaction, the reaction mixture is cooled to ambient temperature and unloaded to afford 865.3 g of light brown reaction product.

Workup

  1. customreaction
  2. customto afford 865.3 g of light brown reaction product

Sources & evidence

ORD record
ord-c767e298f8d84d5eab28785d79eb5157
Source dataset
uspto-grants-2013_10
Patent number
US08557756B2

Reaction notes

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