HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 2,3-Dihydroxybenzoate → Methyl 2-hydroxy-3-(m-tolyloxy)benzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 2,3-Dihydroxybenzoate | HCID 75484 | — |
| Reactant | 3-Tolylboronic acid | HCID 2733950 | — |
| Product | Methyl 2-hydroxy-3-(m-tolyloxy)benzoate | HCID 70926721 | 36.5% |
Reaction Steps
According to the method of (Example 99) <Step 1>, from methyl 2,3-dihydroxybenzoate (1 g) and m-tolyl boronic acid (0.97 g) that are commercially available, the subject compound (0.56 g) was obtained as pale yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08557766B2 |
| Source dataset | uspto-grants-2013_10 |
| ORD ID | ord-4fd9a48650e3414992bdd044b5c1fb59 |
| Source note | uspto-grants-2013_10 |