HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dichloromethane → HCID 178511701, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dichloromethane | HCID 6344 | — |
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 178454064 | HCID 178454064 | — |
| Product | HCID 178511701 | HCID 178511701 | — |
Reaction Steps
A solution of Example 14 step a (196 mg, 0.178 mmol) in TFA (2 mL) and DCM (10 mL) was stirred at RT for 0.5 H, then concentrated in vacuo to give the title compound (quantitative yield). LCMS (Method 2): Rt 0.38 min, m/z 438 [M-CF3CO2+].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08557797B2 |
| Source dataset | uspto-grants-2013_10 |
| ORD ID | ord-c14e57496a90465f83ed0b5bf13ebb0f |
| Source note | uspto-grants-2013_10 |