Tetrahydro-4H-pyran-4-one → HCID 86624999, compound

HRID 1042068Notes

Reaction equation

HRID 1042068 reaction equation
[CH:1]([CH:4]1[CH2:8][CH:7]([C:9](=[O:11])[CH3:10])[CH:6]([CH3:12])[CH2:5]1)([CH3:3])[CH3:2].O1CCC(=O)[CH2:15][CH2:14]1>>[CH:1]([CH:4]1[CH2:8][CH:7]([C:9]([OH:11])([C:14]#[CH:15])[CH3:10])[CH:6]([CH3:12])[CH2:5]1)([CH3:3])[CH3:2]

Participants

3

Reactant 2

HCID 121599Tetrahydro-4H-pyran-4-oneHCID 66743452HCID 66743452, compound

Product 1

HCID 86624999HCID 86624999, compound

Procedure

The title compound was prepared according to the procedures described in Example 6A, substituting 1-(4-isopropyl-2-methylcyclopentyl)ethanone (prepared as described in Roger, A. et al. Bull. Soc. Chim. Fr. 1967, 3030-3037) for tetrahydro-4H-pyran-4-one used in Example 6A.

Workup

  1. customprepared

Sources & evidence

ORD record
ord-9ff4dfa03b524d10bf345b89e99b7ec8
Source dataset
uspto-grants-2013_10
Patent number
US08557828B2

Reaction notes

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