反应详情

In a RBF fitted with a reflux condenser a mixture of diethyl 2-((5-bromopyridin-3-ylamino)methylene)malonate (1 g, 3 mmol) and 1-phenoxybenzene (10 mL, 63 mmol) was heated to reflux for 1 h. The reaction mixture was allowed to cool to RT and CH3CN was added. The resulting solids were filtered and dried to provide the desired product as a light brown solid.

1. customIn a RBF fitted with a reflux condenser
2. temperaturewas heated
3. temperatureto reflux for 1 h
4. filtrationThe resulting solids were filtered
5. customdried