Hydrochloric Acid → HCID 178526855, compound

HRID 1042946Notes

Reaction equation

HRID 1042946 reaction equation
[ClH:1].[N+]([C:5]1[NH:6][CH:7]=[C:8]([N+:10]([O-:12])=[O:11])[N:9]=1)([O-])=O>>[Cl:1][C:5]1[NH:6][CH:7]=[C:8]([N+:10]([O-:12])=[O:11])[N:9]=1

Participants

3

Reactant 2

HCID 313Hydrochloric AcidHCID 178526857HCID 178526857, compound

Product 1

HCID 178526855HCID 178526855, compoundYield 67%

Procedure

In NON-PATENT DOCUMENT 3, after concentrated hydrochloric acid is added to 2,4-dinitroimidazole, the resultant solution is refluxed for 3 hours to perform chlorination reaction, and 2-chloro-4-nitroimidazole is produced at a yield of 67% by performing cooling, filtration and washing.

Workup

  1. customchlorination reaction

Sources & evidence

ORD record
ord-9f71c5e6621243aba6898ca37250ec9e
Source dataset
uspto-grants-2013_10
Patent number
US08558005B2

Reaction notes

Loading…