HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86647915, compound → HCID 67126817, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86647915 | HCID 86647915 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 67126817 | HCID 67126817 | — |
Reaction Steps
A mixture of EXAMPLE 447A (500 mg) and 10% Pd/C (100 mg) in tetrahydrofuran (15 mL) was stirred under H2 for 3 hours. The insoluble material was removed by filtration, and the filtrate was concentrated to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08557983B2 |
| Source dataset | uspto-grants-2013_10 |
| ORD ID | ord-b6f480f501ac4e0caae2538eb72a6a32 |
| Source note | uspto-grants-2013_10 |