Butanal → HCID 86631204, compound

Participants

Reaction Conditions

Reaction Steps

To 263.1 g of N1,N3-dicyclohexyl-1,3-benzenediamine prepared as described in Example 2 were added 59.5 g butyraldehyde, and 2.0 g wet (as received) sulfided platinum on carbon catalyst. The autoclave was pressurized with 4,647 KPa (660 psig) of hydrogen. The reaction was heated to 180° C. over 4 hours, and held at for 180° C. 17 hours. The reaction mass was cooled and filtered, and volatiles were removed by rotary evaporation. The reaction mass was contained and the N1,N3-dicyclohexyl-4-butyl-1,3-benzenediamine was isolated by column chromatography as an oil, 93.5% pure by GCMS analysis. It has the characteristics reported below.

Provenance & Evidence