HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl carbazate → HCID 86686317, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl carbazate | HCID 79242 | — |
| Reactant | 3-Oxotetrahydrofuran | HCID 529392 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 86686317 | HCID 86686317 | 105% |
Reaction Steps
3-oxotetrahydrofuran (5.70 g) was dissolved in methanol (150 mL), and benzyl carbazate (10 g) was added to the solution. The mixture was stirred at room temperature for 12 hours. The reaction mixture was concentrated. 14.8 g of a residue was obtained as a crude purified product. This was used for the next reaction without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08563565B2 |
| Source dataset | uspto-grants-2013_10 |
| ORD ID | ord-e242cff8b09b44d8a1ea590a3b03d261 |
| Source note | uspto-grants-2013_10 |