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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1044383Generated: November 1, 2026

Methanol → HCID 178525737, compound

https://huagongshe.com/reaction/1044383

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMethanolHCID 887—
ReactantHCID 178525738HCID 178525738—
CatalystPalladiumHCID 23938—
ProductHCID 178525737HCID 178525737—

Reaction Steps

Benzyl (5S)-2-[cis-4-(benzoyloxy)cyclohexyl]-1-oxo-2,7-diazaspiro[4.5]decane-7-carboxylate (0.16 g, 0.00033 mol) in methanol (5 mL, 0.1 mol) was stirred with palladium (20 mg, 0.00002 mol) under an atmosphere of hydrogen for 2 h. The mixture was filtered and the filtrate was concentrated to afford the desired product. LC-MS: 357.2 (M+H)+.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08563570B2
Source datasetuspto-grants-2013_10
ORD IDord-7d20c5566f2c4258bdea1dd075b3b822
Source noteuspto-grants-2013_10