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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1044387Generated: October 25, 2026

Methanol → HCID 178477595, compound

https://huagongshe.com/reaction/1044387

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMethanolHCID 887—
ReactantHCID 178477596HCID 178477596—
CatalystPalladiumHCID 23938—
ProductHCID 178477595HCID 178477595—

Reaction Steps

To a solution of benzyl (5S)-1-oxo-2-{trans-4-[(triethylsilyl)oxy]cyclohexyl}-2,7-diazaspiro[4.5]decane-7-carboxylate (2.4 g, 0.0048 mol) in methanol (10 mL, 0.2 mol) was added Pd/C, and the suspension was stirred at rt under a H2 balloon for 1.5 h. The inorganics were filtered and the filtrate was concentrated to afford the desired product.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08563570B2
Source datasetuspto-grants-2013_10
ORD IDord-da8bca61678646aeb0250b4a9ab7955f
Source noteuspto-grants-2013_10