HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 178477595, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | HCID 178477596 | HCID 178477596 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | HCID 178477595 | HCID 178477595 | — |
Reaction Steps
To a solution of benzyl (5S)-1-oxo-2-{trans-4-[(triethylsilyl)oxy]cyclohexyl}-2,7-diazaspiro[4.5]decane-7-carboxylate (2.4 g, 0.0048 mol) in methanol (10 mL, 0.2 mol) was added Pd/C, and the suspension was stirred at rt under a H2 balloon for 1.5 h. The inorganics were filtered and the filtrate was concentrated to afford the desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08563570B2 |
| Source dataset | uspto-grants-2013_10 |
| ORD ID | ord-da8bca61678646aeb0250b4a9ab7955f |
| Source note | uspto-grants-2013_10 |