HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 46910989, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | 1,4-Dioxane hydrochloride | HCID 20443148 | — |
| Reactant | HCID 58580200 | HCID 58580200 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 46910989 | HCID 46910989 | — |
Reaction Steps
To a solution of 4-((4-fluorophenylthio)methyl)-1-(3-methoxy-4-((2-(trimethylsilyl)ethoxy)methoxy)phenyl)pyridin-2(1H)-one Part A (64 mg, 0.13 mmol) in CH2Cl2 (1.0 mL) and MeOH (1.0 mL) was added 4M HCl/Dioxane (2 mL, 8M mmol). After stirring at RT for 2 h, concentration under vacuum provided the crude phenol as a white solid. LC-MS, [M+H]+=358.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08563583B2 |
| Source dataset | uspto-grants-2013_10 |
| ORD ID | ord-3e93bdc9b3f6421a936cb3cf88a9b1dc |
| Source note | uspto-grants-2013_10 |