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HRID1044426

反应详情

EQUATION

反应方程式

HRID 1044426 的结构方程式

REACTANTS

反应物

1
结构：[N-]=[N+]=NCCOCCOCCOCCOCCOCCNC(=O)COCC(=O)O
HCID86619729

未命名化合物

PRODUCTS

生成物

1
结构：NCCOCCOCCOCCOCCOCCNC(=O)COCC(=O)O
HCID86619730

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：O
溶剂HCID962

Water

H2O

PROCEDURE

实验过程

23-Azido-5-oxo-6-aza-3,9,12,15,18,21-hexaoxatricosanoic acid (9.0 g, 21 mmol) was dissolved in water (50 mL) and reduced using H2(g)-Pd/C (10%). The reaction was run until ESI-MS analysis showed complete conversion to the desired product (MH+ calculated: 397.2; found 397.6). The crude product was used in the next step without further purification.