HCID 86619729, compound → 2-{[(17-Amino-3,6,9,12,15-pentaoxaheptadecan-1-yl)carbamoyl]methoxy}acetic acid

Participants

Reaction Steps

23-Azido-5-oxo-6-aza-3,9,12,15,18,21-hexaoxatricosanoic acid (9.0 g, 21 mmol) was dissolved in water (50 mL) and reduced using H2(g)-Pd/C (10%). The reaction was run until ESI-MS analysis showed complete conversion to the desired product (MH+ calculated: 397.2; found 397.6). The crude product was used in the next step without further purification.

Provenance & Evidence