HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetone → N-Isopropylcyclopentanamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetone | HCID 180 | — |
| Reactant | Cyclopentylamine | HCID 2906 | — |
| Catalyst | Palladium hydroxide | HCID 9942167 | — |
| Product | N-Isopropylcyclopentanamine | HCID 17750362 | — |
Reaction Steps
Peariman's catalyst (20% w/w palladium hydroxide-on-carbon) (1.5 g) was added to a solution of cyclopentylamine (15 ml, 0.21 mol) in acetone (200 ml). The reaction mixture was stirred under an atmosphere of hydrogen gas at 414 kPa (60 psi). After stirring for 16 hours the reaction mixture was filtered through Arbocel (trade mark) and the solvent removed under reduced pressure to give the title compound (15 ml) as a thin oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07094769B2 |
| Source dataset | uspto-grants-2006_08 |
| ORD ID | ord-a37b355baf0d4ccb87189a29d7e7e818 |
| Source note | uspto-grants-2006_08 |