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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1044814Generated: November 1, 2026

Nitrogen → HCID 178511559, compound

https://huagongshe.com/reaction/1044814

Reaction equation

Participants

RoleNameHCIDCharge
ReactantNitrogenHCID 947—
ReactantHCID 178523768HCID 178523768—
CatalystPalladiumHCID 23938—
SolventMethanolHCID 887—
ProductHCID 178511559HCID 178511559—

Reaction Steps

In a flame dried round-bottomed flask equipped with a magnetic stir bar and under inert atmosphere (N2), a solution of cis-4-benzyloxycarbonylaminocyclohexane-methanol (235 mg, 0.89 mmol) in MeOH (5 mL) was hydrogenated in the presence of Pd/C (10%) at rt until completion of the reaction. The mixture was then filtered and concentrated under reduced pressure. The title compound was obtained as a colorless oil. LC-MS-conditions 07: tR=0.12 min; [M+H]+=130.26.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08563714B2
Source datasetuspto-grants-2013_10
ORD IDord-2e1e6159d2ac4cabb819fe16c45eb6a2
Source noteuspto-grants-2013_10