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HRID1044856

反应详情

EQUATION

反应方程式

HRID 1044856 的结构方程式

REACTANTS

反应物

3
结构：CC(C)(C)OC(=O)N1CCC(CCBr)CC1
HCID10541625

tert-Butyl 4-(2-bromoethyl)piperidine-1-carboxylate

C12H22BrNO2

结构：CCCCOc1nc(N)c2nc(OC)n(CC3CCN(C(=O)OC(C)(C)C)CC3)c2n1
HCID58306091

未命名化合物

结构：CCCCOc1nc(N)c2nc(OC)[nH]c2n1.O=C(O)C(F)(F)F
HCID178450370

未命名化合物

PRODUCTS

生成物

1
结构：CCCCOc1nc(N)c2nc(OC)n(CCC3CCN(C(=O)OC(C)(C)C)CC3)c2n1
HCID58306196

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CO.ClC(Cl)Cl
溶剂HCID21584188

Chloroform methanol

C2H5Cl3O

PROCEDURE

实验过程

Prepared similarly to Intermediate 13 from 2-butoxy-8-methoxy-9H-purin-6-amine trifluoroacetate salt and 1,1-dimethylethyl 4-(2-bromoethyl)-1-piperidinecarboxylate. TLC chloroform/methanol 9:1:Rf 0.81