HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(5-Methyl-1,2,4-oxadiazol-3-yl)phenyl acetate → 3-(5-Methyl-1,2,4-oxadiazol-3-yl)phenol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(5-Methyl-1,2,4-oxadiazol-3-yl)phenyl acetate | HCID 66797955 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Product | 3-(5-Methyl-1,2,4-oxadiazol-3-yl)phenol | HCID 12042519 | — |
Reaction Steps
A solution of 8.55 g (39.18 mmol) of the product obtained in Step C above in 120 ml of 1N HCl solution is heated at reflux for 90 minutes and is then left at ambient temperature overnight, with stirring. The precipitate is filtered off to yield the title product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08569285B2 |
| Source dataset | uspto-grants-2013_10 |
| ORD ID | ord-10a488ae5abf4fc5897e9468539c7837 |
| Source note | uspto-grants-2013_10 |