HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Toluenesulfonic acid → HCID 19703103, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Toluenesulfonic acid | HCID 6101 | — |
| Reactant | N'-(acetyloxy)-4-iodobenzenecarboximidamide | HCID 86663308 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 19703103 | HCID 19703103 | — |
Reaction Steps
To a solution of the product obtained in Step B above (9.7 g, 31.9 mmol) in 300 ml of toluene there are added 150 mg of para-toluenesulphonic acid and the reaction mixture is heated at reflux, using a Dean-Stark installation, for 24 hours. The mixture is evaporated to dryness and dried using a vacuum pump.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08569285B2 |
| Source dataset | uspto-grants-2013_10 |
| ORD ID | ord-1c06c3c2da6c4d7fbe4542b0c33f260c |
| Source note | uspto-grants-2013_10 |