Triethylamine → HCID 66789652, compound

Participants

Reaction Steps

To a suspension of 13.4 g (0.115 mol) of 2-chloroethylamine hydrochloride in 150 ml of CH2Cl2 there are added 34 ml (0.241 mol) of triethylamine and then, dropwise, 30 g (0.105 mol) of the product obtained in Step A above dissolved in 200 ml of CH2Cl2. The solution is stirred for 2 hours at ambient temperature and is then washed with 1N HCl solution, water and brine. The organic phase is dried over MgSO4 and evaporated. The solid is re-suspended in ethyl ether and filtered off to yield the title product.

Provenance & Evidence