HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,5-Dichloro-nicotinoyl chloride → HCID 86668354, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,5-Dichloro-nicotinoyl chloride | HCID 2799996 | — |
| Reactant | HCID 70498061 | HCID 70498061 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 86668354 | HCID 86668354 | — |
Reaction Steps
57 (50 mg, 0.13 mmol) and 2,5-dichloropyridine-3-carbonyl chloride (29 mg, 0.14 mmol) were suspended in pyridine (1 mL), and stirred overnight at room temperature. The crude product was purified directly via HPLC. LC-MS (M+H=568, obsd.=568).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08569295B2 |
| Source dataset | uspto-grants-2013_10 |
| ORD ID | ord-ab13771656b241d4b19d0e700c0b933b |
| Source note | uspto-grants-2013_10 |