HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Fluorobenzenesulphonyl chloride → HCID 70498545, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Fluorobenzenesulphonyl chloride | HCID 137761 | — |
| Reactant | HCID 70498061 | HCID 70498061 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 70498545 | HCID 70498545 | — |
Reaction Steps
57 (45 mg, 0.11 mmol) and 2-fluorobenzenesulfonyl chloride (24 mg, 0.12 mmol) were suspended in pyridine (1 mL), and stirred overnight at room temperature. The crude product was purified directly via HPLC. LC-MS (M+H=553, obsd.=553).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08569295B2 |
| Source dataset | uspto-grants-2013_10 |
| ORD ID | ord-14688beb4f544a3cbfc9da02a3a66198 |
| Source note | uspto-grants-2013_10 |