HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 58432809, compound → HCID 58432794, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 58432809 | HCID 58432809 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 58432794 | HCID 58432794 | — |
Reaction Steps
To a solution of (±)-benzyl (5-oxo-2-phenyl-1,1′,3′,5-tetrahydrospiro[imidazole-4,2′-inden]-5′-yl)carbamate from Step A (568 mg, 1.94 mmol) in degassed MeOH (2 mL) was added 10% palladium on carbon (5 mg). The suspension was placed under a hydrogen balloon for 3 h, then filtered through a pad of Celite, concentrated, and dried under high vacuum to give the title compound. MS: m/z=278 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08569291B2 |
| Source dataset | uspto-grants-2013_10 |
| ORD ID | ord-89f37d6747a84808af0520b569105d7a |
| Source note | uspto-grants-2013_10 |