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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1045514Generated: October 31, 2026

HCID 58432809, compound → HCID 58432794, compound

https://huagongshe.com/reaction/1045514

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 58432809HCID 58432809—
CatalystPalladiumHCID 23938—
SolventMethanolHCID 887—
ProductHCID 58432794HCID 58432794—

Reaction Steps

To a solution of (±)-benzyl (5-oxo-2-phenyl-1,1′,3′,5-tetrahydrospiro[imidazole-4,2′-inden]-5′-yl)carbamate from Step A (568 mg, 1.94 mmol) in degassed MeOH (2 mL) was added 10% palladium on carbon (5 mg). The suspension was placed under a hydrogen balloon for 3 h, then filtered through a pad of Celite, concentrated, and dried under high vacuum to give the title compound. MS: m/z=278 (M+1).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08569291B2
Source datasetuspto-grants-2013_10
ORD IDord-89f37d6747a84808af0520b569105d7a
Source noteuspto-grants-2013_10