HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 67350918, compound → HCID 58432807, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 67350918 | HCID 67350918 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 58432807 | HCID 58432807 | — |
Reaction Steps
To a solution of (±)-5′-nitro-2-propyl-1′,3′-dihydrospiro[imidazole-4,2′-inden]-5(1H)-one from Step A (20.0 mg, 0.073 mmol) in degassed MeOH (5 mL) was added 10% palladium on carbon (10 mg). The suspension was placed under a hydrogen balloon for 1 h, then filtered through a pad of Celite, concentrated, and dried under high vacuum to give the title compound. MS: m/z=244 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08569291B2 |
| Source dataset | uspto-grants-2013_10 |
| ORD ID | ord-df56809f6739464bb9199ec214d14ce6 |
| Source note | uspto-grants-2013_10 |