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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1045520Generated: November 1, 2026

HCID 67389382, compound → HCID 58432798, compound

https://huagongshe.com/reaction/1045520

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 67389382HCID 67389382—
CatalystPalladiumHCID 23938—
SolventMethanolHCID 887—
ProductHCID 58432798HCID 58432798—

Reaction Steps

To a solution of (±)-2-tert-butyl-5′-nitro-1′,3′-dihydrospiro[imidazole-4,2′-inden]-5(1H)-one from Step B (22.0 mg, 0.077 mmol) in degassed MeOH (5 mL) was added 10% palladium on carbon (10 mg). The suspension was placed under a hydrogen balloon for 1 h, then filtered through a pad of Celite, concentrated, and dried under high vacuum to give the title compound. MS: m/z=258 (M+1).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08569291B2
Source datasetuspto-grants-2013_10
ORD IDord-bdb257c34bc242418aeff05a77020ddb
Source noteuspto-grants-2013_10