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HRID1046385

反应详情

EQUATION

反应方程式

HRID 1046385 的结构方程式

REACTANTS

反应物

3
结构：[Na+].[OH-]
HCID14798

Sodium Hydroxide

HNaO

结构：N#C[O-].[Na+]
HCID517096

Cyanic acid, sodium salt

CNNaO

结构：C=CCc1c(O)ccc(NCc2ccccc2)c1C(=O)c1ccc(C(C)C)cc1
HCID45141177

未命名化合物

PRODUCTS

生成物

1
结构：C=CCc1c(O)ccc2c1c(-c1ccc(C(C)C)cc1)nc(=O)n2Cc1ccccc1
HCID45141389

6-Hydroxy-4-[4-(1-methylethyl)phenyl]-1-(phenylmethyl)-5-(2-propen-1-yl)-2(1H)-quinazolinone

C27H26N2O2

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CC(=O)O
溶剂HCID176

Acetic Acid

C2H4O2

PROCEDURE

实验过程

A solution of 15 mg (39 μmol) (2-allyl-6-benzylamino-3-hydroxy-phenyl)-(4-isopropyl-phenyl)-methanone and 2.5 mg sodium cyanate in 0.2 ml acetic acid is stirred at r.t. for 16 h. Aqueous sodium hydroxide solution is added and the product is extracted with dichloromethane.

WORKUP

后处理

  1. extractionthe product is extracted with dichloromethane