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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1046958Generated: November 2, 2026

HCID 152764707, compound → HCID 141621175, compound

https://huagongshe.com/reaction/1046958

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 152764707HCID 152764707—
CatalystPalladiumHCID 23938—
SolventMethanolHCID 887—
ProductHCID 141621175HCID 141621175100%

Reaction Steps

3,5-bis-(N,N′-bis-Boc-guanidinyl)methyl nitrobenzene (4.52 g, 6.86 mmol) was dissolved in 50 ml absolute methanol, and catalytic amount of Pd/C was added into this mixture. The mixture was stirred at room temperature under hydrogen atmosphere for four hours. The solvent was removed to give the title compound as a light yellow solid (100%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08569451B2
Source datasetuspto-grants-2013_10
ORD IDord-72f0b0de950046c99015afc3001213d3
Source noteuspto-grants-2013_10