HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 152764707, compound → HCID 141621175, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 152764707 | HCID 152764707 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 141621175 | HCID 141621175 | 100% |
Reaction Steps
3,5-bis-(N,N′-bis-Boc-guanidinyl)methyl nitrobenzene (4.52 g, 6.86 mmol) was dissolved in 50 ml absolute methanol, and catalytic amount of Pd/C was added into this mixture. The mixture was stirred at room temperature under hydrogen atmosphere for four hours. The solvent was removed to give the title compound as a light yellow solid (100%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08569451B2 |
| Source dataset | uspto-grants-2013_10 |
| ORD ID | ord-72f0b0de950046c99015afc3001213d3 |
| Source note | uspto-grants-2013_10 |