HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1046991Generated: October 25, 2026
Aminoacetaldehyde dimethyl acetal → HCID 178495885, compound
https://huagongshe.com/reaction/1046991
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Aminoacetaldehyde dimethyl acetal | HCID 89728 | — |
| Reactant | 5,11-dihydro-6H-pyrido[2,3-b][1,4]benzodiazepine-6-thione | HCID 45496229 | — |
| Product | HCID 178495885 | HCID 178495885 | — |
Reaction Steps
A mixture of 5,11-dihydro-6H-pyrido[2,3-b][1,4]benzodiazepine-6-thione (3.21 g, 14 mmol) and 2,2-dimethoxyethylamine (7.6 mL, 70 mmol) was heated to 95° C. for 1 hour. After cooling to room temperature the solvent was evaporated in vacuo. The crude product was used in the next step without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08569331B2 |
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| Source dataset | uspto-grants-2013_10 |
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| ORD ID | ord-1ddb5d730f7a48b5a2e2bc5cae496d22 |
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| Source note | uspto-grants-2013_10 |
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