HuagongsheHuagongshe Chemistry Print Report · For research reference only
(Pyridin-4-yl)boronic acid → HCID 67503588, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (Pyridin-4-yl)boronic acid | HCID 2734379 | — |
| Reactant | HCID 136390213 | HCID 136390213 | — |
| Product | HCID 67503588 | HCID 67503588 | — |
Reaction Steps
The title compound was synthesized according to the procedure described in step 1 of example 19 using 2-bromo-3-phenyl-9H-benzo[f]imidazo[1,2-d]pyrido[2,3-b][1,4]diazepine and pyridin-4-ylboronic acid. 1HNMR (CDCl3) 400 MHz δ: 8.50-8.47 (m, 2H), 8.18-8.14 (m, 1H), 8.06-8.03 (m, 1H), 7.49-7.46 (m, 2H), 7.44-7.31 (m, 5H), 7.29-7.22 (m, 1H), 7.20-7.16 (m, 1H), 6.98-6.94 (m, 1H), 6.83-6.78 (m, 1H), 6.64 (dd, J=8.0, 4.6 Hz, 1H), 6.28 (br s, 1H); LC/MS: 388 [M+H].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08569331B2 |
| Source dataset | uspto-grants-2013_10 |
| ORD ID | ord-0aa2dd444a984e118df877c9ece108b5 |
| Source note | uspto-grants-2013_10 |