HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine hydrate (1:1) → HCID 58242743, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Reactant | 4H,4H-Perfluoro-6,6-dimethylheptane-3,5-dione | HCID 75067 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 58242743 | HCID 58242743 | 79.5% |
Reaction Steps
At room temperature, hydrazine hydrate (2.06 g) is added to a solution of 1,1,1,2,2-pentafluoro-6,6-dimethylheptane-3,5-dione (10.1 g) in ethanol (100 ml). The reaction mixture is stirred at room temperature overnight. After removal of the solvents under reduced pressure, 3-tert-butyl-5-(pentafluoroethyl)-1H-pyrazole (7.9 g, 79%) is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08569509B2 |
| Source dataset | uspto-grants-2013_10 |
| ORD ID | ord-4a2c7da832f04340ba0f85ef63d0ae1f |
| Source note | uspto-grants-2013_10 |