HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxalyl chloride → HCID 21390659, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | Benzoic acid, 4-(azidosulfonyl)- | HCID 86999 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 21390659 | HCID 21390659 | — |
Reaction Steps
Under Argon at 0° C. and while stiffing, 0.7 ml oxalylchloride were added dropwise to a suspension of 908 mg (4 mmol) 4-carboxybenzene sulfonyl azide (Aldrich). The mixture was allowed to warm to room temperature. Then, 10 μl DMF (dimethylformamide) were added. After stirring for 1 h at room temp. a clear solution was formed. The solvent was removed using a rotary evaporator.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08569515B2 |
| Source dataset | uspto-grants-2013_10 |
| ORD ID | ord-bc5e0c51a7e840eb8ab098d4faea2839 |
| Source note | uspto-grants-2013_10 |