HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-tert-Butylcyclohexanone → Morpholine, 4-[4-(1,1-dimethylethyl)-1-cyclohexen-1-yl]-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-tert-Butylcyclohexanone | HCID 7392 | — |
| Reactant | Morpholine | HCID 8083 | — |
| Reactant | Morpholine, 4-(1-cyclohexen-1-yl)- | HCID 69589 | — |
| Solvent | Cyclohexane | HCID 8078 | — |
| Product | Morpholine, 4-[4-(1,1-dimethylethyl)-1-cyclohexen-1-yl]- | HCID 11356517 | — |
Reaction Steps
Compound III′ (white solid) is obtained quantitatively according to Example 1, from 4-tert-butylcyclohexanone (77.12 g, 0.50 mol), morpholine (54.01 g, 0.62 mol) and cyclohexane (60 mL).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08569518B2 |
| Source dataset | uspto-grants-2013_10 |
| ORD ID | ord-cc591e3d936c49819385ad7a920d4d27 |
| Source note | uspto-grants-2013_10 |