HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 23134613, compound → 3-Ethoxy-2-methylaniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 23134613 | HCID 23134613 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 3-Ethoxy-2-methylaniline | HCID 13737011 | — |
Reaction Steps
A mixture of 1-ethoxy-2-methyl-3-nitrobenzene described in Reference Preparation example 2539.9 g, palladium-carbon (palladium 5%) 4 g and ethanol 200 mL was stirred at room temperature under hydrogen atmosphere for eighteen hours. The mixtures were filtered and the filtrates were concentrated to give 3-ethoxy-2-methylaniline 33.0 g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09380782B2 |
| Source dataset | uspto-grants-2016_07 |
| ORD ID | ord-0124a7c0ff9a437f91fc0767421e3bb0 |
| Source note | uspto-grants-2016_07 |