HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydroxyamine hydrochloride → HCID 77843991, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydroxyamine hydrochloride | HCID 443297 | — |
| Reactant | Sodium Methoxide | HCID 10942334 | — |
| Reactant | HCID 178503887 | HCID 178503887 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 77843991 | HCID 77843991 | — |
Reaction Steps
Sodium methanolate (9.26 ml, 4.63 mmol, Eq: 3.00) was added into a solid hydroxylamine hydrochloride (322 mg, 4.63 mmol, Eq: 3.00) at rt. Stirred at rt for 0.5 hrs, a solution of (Z)-methyl N′-cyano-N-(3-(trifluoromethyl)phenyl)carbamimidothioate (400 mg, 1.54 mmol, Eq: 1.00) in ethanol was added and the mixture was heated to 63° C. overnight.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09382218B2 |
| Source dataset | uspto-grants-2016_07 |
| ORD ID | ord-436900bf989e4799ae1a091bb4954f31 |
| Source note | uspto-grants-2016_07 |