Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Iodine | HCID 807 | — |
| Reactant | 10H-Phenothiazine, 1-ethyl- | HCID 5257546 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 87410566 | HCID 87410566 | — |
Reaction Steps
1-Ethyl-10H-phenothiazine (646 mg, 2.84 mmol) was dissolved in CHCl3 (10 mL) and cooled to 0° C. as a solution of Iodine (2.16 g, 8.51 mmol) dissolved in CHCl3 (50 mL) was added dropwise. The mixture was stirred at 0° C. for 2 h, then allowed to warm to RT overnight.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US09382221B2 |
|---|
| Source dataset | uspto-grants-2016_07 |
|---|
| ORD ID | ord-c0839109fa6644149ac231e8e11bfdf7 |
|---|
| Source note | uspto-grants-2016_07 |
|---|
